Gas chromatography and mass spectrometry [electronic resource] : a practical guide / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson.

By: Sparkman, O. David (Orrin David), 1942-Contributor(s): Penton, Zelda | Kitson, Fulton G | ProQuest (Firm)Material type: TextTextPublication details: Boston : Elsevier, 2011Edition: 2nd edDescription: xix, 611 p. : ill. (some col.)ISBN: 9780080920153 (electronic bk.)Subject(s): Gas chromatography | Mass spectrometryGenre/Form: Electronic books.DDC classification: 543/.85 LOC classification: QD79.C45 | S66 2011Online resources: Click to View
Contents:
The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures.
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Includes bibliographical references and index.

The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures.

Electronic reproduction. Ann Arbor, MI : ProQuest, 2016. Available via World Wide Web. Access may be limited to ProQuest affiliated libraries.

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